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International Journal of Nano Dimension، جلد ۶، شماره ۴، صفحات ۴۰۱-۴۰۷
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عنوان فارسی |
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چکیده فارسی مقاله |
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کلیدواژههای فارسی مقاله |
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عنوان انگلیسی |
Synthesis and characterization of Nickel (II) Chloride nanoparticles with the study of their thermal behavior |
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چکیده انگلیسی مقاله |
In this research nanoparticles of Nickel (II) Chloride were synthesized and characterized using fourier transform infrared (FT-IR) spectra. Nanoparticles of Nickel (II) Chloride were prepared by using of ball mill device. A ball mill is one kind of grinding machine, and it is a device in which media balls and solid materials (the materials to be ground) are placed in a container. In the research Nickel (II) Chloride compound was milled for 10 h at 250 rpm in a hardened stainless steel medium. The resulting nanoparticles were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The SEM imaging technique was applied for the observation of grain sizes and the morphology of the nanoparticles. The Debye-Scherrer formula was used to confirm the grain sizes determined by the SEM slides. XRD results of nanoparticles showed that the crystallite size of reaching 59 mm after 10 h at 250 RPM. Thermal behavior of nanoparticles was considered by using of DTA /TGA thermal analysis device. TGA analysis reveals that the synthesized Nickel (II) Chloride nanoparticle was thermally stable up to 900°C. |
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کلیدواژههای انگلیسی مقاله |
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نویسندگان مقاله |
z رحمانی | department of chemistry, takestan branch, islamic azad university,takestan , iran. سازمان اصلی تایید شده: دانشگاه آزاد اسلامی علوم و تحقیقات (Islamic azad university science and research branch)
sh غمامی | department of chemistry, faculty of science, imam khomeini international university, qazvin, iran. سازمان اصلی تایید شده: دانشگاه بین المللی امام خمینی (Imam khomeini international university)
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نشانی اینترنتی |
http://www.ijnd.ir/article_12801_710c7fe14d31a31004a739ce6eba1bb9.pdf |
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زبان مقاله منتشر شده |
en |
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