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JCR 2016
جستجوی مقالات
جمعه 18 مهر 1404
Nanomedicine Journal
، جلد ۲، شماره ۴، صفحات ۲۶۹-۲۷۲
عنوان فارسی
چکیده فارسی مقاله
کلیدواژههای فارسی مقاله
عنوان انگلیسی
Synthesis of graphene oxide-TiO2 nanocomposite as an adsorbent for the enrichment and determination of rutin
چکیده انگلیسی مقاله
Objective(s): In our study, graphene oxide-TiO2 nanocomposite (GO/TiO2) was prepared and used for the enrichment of rutin from real samples for the first time. Materials and Methods: The synthesized GO/TiO2 was characterized by X-ray diffraction, scanning electron microscopy, and FT-IR spectra. The enrichment process is fast and highly efficient. The factors including contact time, pH, and amount of GO/TiO2 affecting the adsorption process were studied. Results: The maximum adsorption capacity for ciprofloxacin was calculated to be 59.5 mg/g according to the Langmuir adsorption isotherm. The method yielded a linear calibration curve in the concentration ranges from 15 to 200 μg/L for the rutin with regression coefficients (r2) of 0.9990. The limits of detection (LODs, S/N=3) and limits of quantification (LOQs, S/N=10) were found to be 8 μg/Land 28 μg/L, respectively. Both the intra-day and inter-day precisions (RSDs) were < 10% . Conclusion: The developed approach offered wide linear range, and good reproducibility. Owing to the diverse structures and unique characteristic, GO/TiO2 possesses great potential in the enrichment and analysis of trace rutin in real aqueous samples.
کلیدواژههای انگلیسی مقاله
Enrichment, GO-TiO2, Nanocomposite, Rutin
نویسندگان مقاله
محمدرضا گایینی | mohammad reza gaeeni
laser and optics research school, nuclear science and technology research institute, aeoi, north karegar, tehran, iran|photonic laboratory, physics department, kharazmi university,tehran, iran
مرضیه توحیدیان | marzieh tohidian
faculty of medicine, tehran university of medical sciences, pour-sina ave, tehran, iran
سازمان اصلی تایید شده
: دانشگاه علوم پزشکی تهران (Tehran university of medical sciences)
مرتضی ساسانی قمصری | morteza sasani ghamsari
laser and optics research school, nuclear science and technology research institute, aeoi, north karegar, tehran, iran
محمد حسین مجلس آرا | mohammad hossein majles ara
photonic laboratory, physics department, kharazmi university,tehran, iran
نشانی اینترنتی
http://nmj.mums.ac.ir/article_4958.html
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en
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