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Iranian Journal of Public Health، جلد ۳۸، شماره ۱، صفحات ۸۹-۹۹
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عنوان انگلیسی Trace Analysis of Xylene in Occupational Exposures Monitoring
چکیده انگلیسی مقاله Background: Determination of organic pollutants usually requires extraction of the pollutants from samples, using hazard­ous solvent. Solid phase micro-extraction (SPME) is a solvent-free equilibrium extraction method, in which, proper calibra­tion can allow quantitative measurements of organic pollutants at a very good sensitivity without the use of any organic sol­vent. Because individual VOCs are generally present in urine only at trace levels, a sensitive and accurate determination technique is essential. Methods: This study describes the optimization of headspace solid phase micro-extraction (HS-SPME) followed by gas chromatography equipped with flame ionization detector (GC-FID) for xylene in spiked urine. Through this investigation, the parameters affecting the extraction and GC determination of xylene, including extraction time, temperature, desorption temperature, desorption time, salt addition, sample pH, sample volume and sample agitation were studied. Results: An op­timized headspace extraction was carried out at 30°C for 6 min in presence of 0.2 gml -1 of NaCl in the sample solution. De­sorption of the xylene was carried out for 60 sec. at 250°C. The optimized procedure was also validated with three different pools of spiked urine samples and showed a good reproducibility over six consecutive days as well as six within-day ex­periments. In this study, the accuracy, linearity, and detection limits were also determined. Conclusion: The HS-SPME-GC-FID technique provided a relatively simple, convenient, practical procedure, which can be successfully applied for determination of xylene in spiked urine when an occupational exposure monitoring is required.
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نویسندگان مقاله hr حیدری | hr heidari
dept. of occupational health


sj شاه طاهری | sj shahtaheri
dept. of occupational health, center for environmental research


m علی محمدی | m alimohammadi
dept .of environmental health


a رحیمی فروشانی | a rahimi froshani
dept. of epidemiology and biostatistics, school of public health, tehran university of medical scien

سازمان اصلی تایید شده: دانشگاه تهران (Tehran university)

نشانی اینترنتی http://ijph.tums.ac.ir/index.php/ijph/article/view/3216
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زبان مقاله منتشر شده en
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